A simple method of purifying authigenic 10Be from sediments for AMS-analysis


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Julia.Loftifield [ at ] awi.de

Abstract

The cosmogenic radionuclide 10Be is used for a variety of applications, its analysis however requires laborious purification methods. We developed a simple purification protocol for Be from sediment samples that works without strongly hazardous chemicals or time consuming and expensive ion exchange columns. The combination of hydroxide precipitations and precipitation in NaHCO3 was compared to an established protocol of hydroxide precipitations and ion exchange columns. The new method has a slightly lower Be-yield and purity of the resulting samples. However, this does not have a significant influence on performance during AMS-measurement where both methods performed equally well. The avoidance of column chromatography reduces sample preparation costs and space requirements in the lab allowing for more samples to be prepared simultaneously.



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Eprint ID
59206
DOI 10.1016/j.nimb.2023.165179

Cite as
Loftfield, J. , Lachner, J. , Malter, M. , Stübner, K. and Adolphi, F. (2024): A simple method of purifying authigenic 10Be from sediments for AMS-analysis , Nuclear Instruments and Methods in Physics Research Section B Beam Interactions with Materials and Atoms, 547 , p. 165179 . doi: 10.1016/j.nimb.2023.165179


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